Skip to main content

Renin Angiotensin Mechanism.

Forced Circulation Evaporators.

 

Definition:

  • The equipment used for carrying out the process of evaporation are called “Evaporators”.

  • Evaporators are classified according to the form of the heat movement,

    • Natural circulation evaporators. e.g Evaporating Pan.

    • Forced circulation evaporation. e.g. Modified evaporating pan.

    • Film evaporators. e.g Climbing film evaporator.

FORCED CIRCULATION EVAPORATORS:

  • Forced circulation evaporators are natural circulation evaporators with some added form of mechanical agitation. Different forms of forced circulation evaporators can be designed.

  • An evaporating pan, in which the contents are agitated by a stirring rod or pole could be described as a forced circulation evaporator.

  • A mechanically operated propeller or paddle agitator can be introduced into an evaporating pan or still.

  • Propeller or paddle agitator can be introduced into the downtake of a short-tube evaporator.

  • A typical forced circulation evaporator can be shown as follows:


Construction:

  • The evaporator consists of a short tube calandria and a large cylindrical vessel (body of the evaporator) for separation of vapor and liquid. 

  • The liquor inlet is provided at the side of the cylindrical vessel. 

  • A pump is fitted in between the calandria and the body of the evaporator. 

  • A tangential inlet for liquid under high pressure is placed at the neck of the body of the evaporator. 

  • The vapor outlet is placed at the top of the body and it may be passed through a condenser to collect the condensed liquid.

Working Principle:

  • Feed is introduced through the liquor inlet. 

  • Pump will force the liquid through the calandria. 

  • Steam heats the liquid inside the calandria. 

  • As it is under pressure in the tubes the boiling point is elevated and no boiling takes place. 

  • As the liquor leaves the tubes and enters the body of the evaporator through the tangential inlet there is a drop in pressure and vapor flashes off from the superheated liquor. 

  • The concentrated liquid is pumped out through the product outlet and the vapor is collected through the vapor outlet.

Advantages

  1. Rapid liquid movement improves heat transfer, especially with viscous liquids or materials that deposit solids or foam readily.

  2. The forced circulation overcomes the effect of greater viscosity of liquids when evaporated under reduced pressure.

  3. Rapid evaporation rate makes this method suitable for thermolabile materials, e.g. it is used in practice for the concentration of insulin and liver extracts

Commonly Asked Questions.

  1. Define evaporation and write a short note on “Forced Circulation Evaporators.”.

  2. With help of a well labelled diagram, describe construction and working of “Forced Circulation Evaporators”.

Popular posts from this blog

Rate of Drying Curve.

  Definition Drying is defined as the removal of liquid from a product usually with application of heat. Rate of Drying Curve. Drying process can be divided into three periods Initial Adjustment Period. Constant drying rate period. First falling drying rate period. Second falling rate period. Initial Adjustment Period (A-B): Also called the “ Heating up” period . In this period the substance gets heat and increases in temperature. Drying has not yet started. Constant drying rate period (B-C): During this period the temperature of the solid and the rate of drying remain constant. The moisture evaporating from the surface is replaced by water diffusing from the interior of the solid at a rate equal t o the rate of evaporation.  The moisture content at the end of constant rate (point C) is referred to as the critical moisture content (CMC).  At CMC, dry spots start appearing and drying rate starts falling . First falling drying rate period (C-D): This period is also called ...

Heat Exchangers and Heat Interchangers.

  In pharmaceutical industries many types of equipments are used for transfer of heat, they can be classified as follows, Heat Exchangers. Heat Interchangers. Heat Exchangers: These devices are used for transferring heat from a fluid (Hot Gas or Steam) to another fluid (Liquid) through a metal wall. Heat Interchangers: These devices are used for transferring heat from a One liquid to another liquid or one gas to another gas through a metal wall. HEAT EXCHANGERS; The equipment used for heat transferring are known as heat exchangers. Some of the processes that involves heat transfer in pharmaceutical industries are: Preparation of starch paste (in steam jacketed kettle). Crystallization. Evaporation. Distillation.  Classification of heat exchangers On the basis of transfer of heat, heat exchangers are classified as: Direct transfer type:  The hot and cold fluids are separated by a metal wall through which the heat is transferred from hot fluid to cold fluid. E.g. shell and ...

Flash Distillation.

  Principle: When a hot mixture is allowed to enter from a high-pressure zone into a low pressure zone, the entire liquid mixture is suddenly vaporized. This process is known as flash vaporization .  During this process, the chamber is cooled.  The less volatile fraction is condensed and the more volatile component remains in the vapor phase .  This process requires time, hence liquid and vapor are kept in intimate contact until equilibrium is achieved. Flash distillation is also called equilibrium distillation because separation of two liquids takes place when liquid and vapor phases are at equilibrium. Equipment used for Flash Distillation: Construction: It consists of a pump, which is connected to a feed reservoir.  Pumps help in pumping the feed into the heating chamber.  The heating chamber is heat supplied by steam.  The other end of the pipe is directly introduced into the vapor-liquid separator through a reducing valve.  The vapor outlet...